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Monitoring phthalates in table and fortified wines by headspace solid-phase microextraction combined with gas chromatography–mass spectrometry analysis

2020Journal article Open access
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dc.contributor.authorPerestrelo, Rosa
dc.contributor.authorSilva, Catarina L.
dc.contributor.authorAlgarra, Manuel
dc.contributor.authorCâmara, José S.
dc.date.accessioned2022-01-04T15:49:31Z
dc.date.available2022-01-04T15:49:31Z
dc.date.issued2020
dc.description.abstractPhthalates are a class of endocrine disruptors extensively used in plastic production as plasticizers, and as a result, they can be found in foods as a result of their migration ability. The occurrence of phthalates was monitored in 20 Portuguese wines using a simple, reliable, and environmentally friendly analytical method, headspace solid-phase microextraction combined with gas chromatography−mass spectrometry. Satisfactory figures of merit of method, linearity (correlation coefficient of ≥0.992), recovery (80.3−107.6%), precision (relative standard deviation of <13%), and limits of detection (0.03−0.11 μg/L) and quantification (0.09−0.36 μg/L) were achieved. Dibutyl phthalate and di-n-octyl phthalate were found in measurable quantities in table and fortified wines. The obtained results revealed that these wines do not represent any concern for human exposure, because their concentrations were lower than the tolerable daily intakes established by the European Food Safety Authority.pt_PT
dc.description.versioninfo:eu-repo/semantics/publishedVersionpt_PT
dc.identifier.citationPerestrelo, R., Silva, C. L., Algarra, M., & Câmara, J. S. (2020). Monitoring phthalates in table and fortified wines by headspace solid-phase microextraction combined with gas chromatography–mass spectrometry analysis. Journal of Agricultural and Food Chemistry, 68(31), 8431-8437. https://doi.org/10.1021/acs.jafc.0c02941pt_PT
dc.identifier.doi10.1021/acs.jafc.0c02941pt_PT
dc.identifier.urihttp://hdl.handle.net/10400.13/3946
dc.language.isoengpt_PT
dc.peerreviewedyespt_PT
dc.publisherAmerican Chemical Societypt_PT
dc.relationMadeira Chemistry Research Centre
dc.relationMadeira Chemistry Research Centre
dc.rights.urihttp://creativecommons.org/licenses/by-nc-nd/4.0/pt_PT
dc.subjectPhthalatespt_PT
dc.subjectWinespt_PT
dc.subjectHS−SPME/GC−MSpt_PT
dc.subjectRisk exposurept_PT
dc.subject.pt_PT
dc.subjectFaculdade de Ciências Exatas e da Engenhariapt_PT
dc.subjectCentro de Química da Madeira
dc.titleMonitoring phthalates in table and fortified wines by headspace solid-phase microextraction combined with gas chromatography–mass spectrometry analysispt_PT
dc.typejournal article
dspace.entity.typePublication
oaire.awardTitleMadeira Chemistry Research Centre
oaire.awardTitleMadeira Chemistry Research Centre
oaire.awardURIinfo:eu-repo/grantAgreement/FCT/6817 - DCRRNI ID/UIDB%2F00674%2F2020/PT
oaire.awardURIinfo:eu-repo/grantAgreement/FCT/6817 - DCRRNI ID/UIDP%2F00674%2F2020/PT
oaire.citation.endPage8437pt_PT
oaire.citation.issue31pt_PT
oaire.citation.startPage8431pt_PT
oaire.citation.titleJournal of Agricultural and Food Chemistrypt_PT
oaire.citation.volume68pt_PT
oaire.fundingStream6817 - DCRRNI ID
oaire.fundingStream6817 - DCRRNI ID
person.familyNamePerestrelo
person.familyNameSousa Luís
person.familyNameCâmara
person.givenNameRosa
person.givenNameCatarina Grace
person.givenNameJosé
person.identifier1441319
person.identifierC-1300-2019
person.identifierG-3003-2013
person.identifier.ciencia-id251A-D5F7-9E32
person.identifier.ciencia-id9813-3B88-BA8D
person.identifier.ciencia-id481C-08CE-90E5
person.identifier.orcid0000-0002-7223-1022
person.identifier.orcid0000-0002-3018-3165
person.identifier.orcid0000-0003-1965-3151
person.identifier.ridI-2307-2014
person.identifier.scopus-author-id16686828800
person.identifier.scopus-author-id57194492726
person.identifier.scopus-author-id10140393000
project.funder.identifierhttp://doi.org/10.13039/501100001871
project.funder.identifierhttp://doi.org/10.13039/501100001871
project.funder.nameFundação para a Ciência e a Tecnologia
project.funder.nameFundação para a Ciência e a Tecnologia
rcaap.rightsopenAccesspt_PT
rcaap.typearticlept_PT
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