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Microextraction using packed sorbent as an effective and high-throughput sample extraction technique: recent applications and future trends

2013Journal article Open access
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dc.contributor.authorPereira, J.
dc.contributor.authorGonçalves, J.
dc.contributor.authorAlves, V.
dc.contributor.authorCâmara, J. S.
dc.date.accessioned2021-12-02T14:46:03Z
dc.date.available2021-12-02T14:46:03Z
dc.date.issued2013
dc.description.abstractIn the last decade, several developments, particularly in the liquid chromatography and hyphenated techniques fields, have allowed researchers to reach analytical limits that are becoming very close to the single molecule level. Sample preparation, however, despite being a key step in the analytical methodology, did not track these developments and very few approaches able to cope with these stringent analytical requirements were developed. One such approach is microextraction by packed sorbent (MEPS), a sophisticated and miniaturized form of solid phase extraction that has reduced to the microliter scale every step of the sample extraction methodology including sample volume and solvent usage. Simultaneously, the amount of extraction phase used was also reduced and, more importantly, the sorbent is reusable dozens of times which significantly lowers the cost of analysis versus other solid-phase extraction approaches. In this review, we will update the state-of-the-art of the MEPS technique, focusing on the trends and applications reported since 2010 and future perspectives and developments that in our view will further improve the high-throughput potential and applications of this sample preparation methodology.pt_PT
dc.description.versioninfo:eu-repo/semantics/publishedVersionpt_PT
dc.identifier.citationPereira, J., Gonçalves, J., Alves, V., & Câmara, J. S. (2013). Microextraction using packed sorbent as an effective and high-throughput sample extraction technique: recent applications and future trends. Sample Preparation, 1(2013), 38-53.• DOI: 10.2478/sampre-2013-0005pt_PT
dc.identifier.doi10.2478/sampre-2013-0005pt_PT
dc.identifier.urihttp://hdl.handle.net/10400.13/3880
dc.language.isoengpt_PT
dc.peerreviewedyespt_PT
dc.publisherDe Gruyterpt_PT
dc.rights.urihttp://creativecommons.org/licenses/by/4.0/pt_PT
dc.subjectMicroextraction by packed sorbent (MEPS)pt_PT
dc.subjecteVolpt_PT
dc.subjectSample preparationpt_PT
dc.subjectSolid phase extraction (SPE)pt_PT
dc.subject.pt_PT
dc.subjectFaculdade de Ciências Exatas e da Engenhariapt_PT
dc.subjectCentro de Química da Madeira
dc.titleMicroextraction using packed sorbent as an effective and high-throughput sample extraction technique: recent applications and future trendspt_PT
dc.typejournal article
dspace.entity.typePublication
oaire.citation.endPage53pt_PT
oaire.citation.issue1pt_PT
oaire.citation.startPage38pt_PT
oaire.citation.titleSample Preparationpt_PT
oaire.citation.volume5pt_PT
person.familyNameAugusto Machado Pereira
person.familyNameGonçalves
person.familyNameAlves
person.familyNameCâmara
person.givenNameJorge
person.givenNameJoão
person.givenNameVera
person.givenNameJosé
person.identifierG-3003-2013
person.identifier.ciencia-idEC12-EE8F-50E8
person.identifier.ciencia-id8C14-3188-9E44
person.identifier.ciencia-idE515-0AFA-CB1D
person.identifier.ciencia-id481C-08CE-90E5
person.identifier.orcid0000-0003-0316-5348
person.identifier.orcid0000-0002-1265-6686
person.identifier.orcid0000-0002-1485-6032
person.identifier.orcid0000-0003-1965-3151
person.identifier.ridC-1348-2019
person.identifier.scopus-author-id52163735200
person.identifier.scopus-author-id55792994000
person.identifier.scopus-author-id10140393000
rcaap.rightsopenAccesspt_PT
rcaap.typearticlept_PT
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relation.isAuthorOfPublication7971c475-3f08-4462-96b1-79e96c9615a4
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relation.isAuthorOfPublication.latestForDiscovery2f4d7adf-ab6b-40ab-85d5-73995a784bda

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