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In situ biosynthesis of bacterial nanocellulose-CaCO3 hybrid bionanocomposite: one-step process

dc.contributor.authorMohammadkazemi, Faranak
dc.contributor.authorFaria, Marisa
dc.contributor.authorCordeiro, Nereida
dc.date.accessioned2021-04-30T13:07:08Z
dc.date.available2021-04-30T13:07:08Z
dc.date.issued2016
dc.description.abstractIn this work, a simple and green route to the synthesis of the bacterial nanocellulose-calcium carbonate (BNC/CaCO3) hybrid bionanocomposites using one-step in situ biosynthesis was studied. The CaCO3 was incorporated in the bacterial nanocellulose structure during the cellulose biosynthesis by Gluconacetobacter xylinus PTCC 1734 bacteria. Hestrin-Schramm (HS) and Zhou (Z) culture media were used to the hybrid bionanocomposites production and the effect of ethanol addition was investigated. Attenuated total reflection Fourier transform infrared spectroscopy, field emission scanning electron microscopy, X-ray diffraction, energy-dispersive X-ray spectroscopy, inverse gas chromatography and thermogravimetric analysis were used to characterize the samples. The experimental results demonstrated that the ethanol and culture medium play an important role in the BNC/CaCO3 hybrid bionanocomposites production, structure and properties. The BNC/CaCO3 biosynthesized in Z culture medium revealed higher O/C ratio and amphoteric surface character, which justify the highest CaCO3 content incorporation. The CaCO3 was incorporated into the cellulosic matrix decreasing the bacterial nanocellulose crystallinity. This work reveals the high potential of in situ biosynthesis of BNC/CaCO3 hybrid bionanocomposites and opens a new way to the high value-added applications of bacterial nanocellulose.pt_PT
dc.description.versioninfo:eu-repo/semantics/publishedVersionpt_PT
dc.identifier.citationMohammadkazemi, F., Faria, M., & Cordeiro, N. (2016). In situ biosynthesis of bacterial nanocellulose-CaCO3 hybrid bionanocomposite: One-step process. Materials Science and Engineering: C, 65, 393-399.pt_PT
dc.identifier.doi10.1016/j.msec.2016.04.069pt_PT
dc.identifier.urihttp://hdl.handle.net/10400.13/3336
dc.language.isoengpt_PT
dc.peerreviewedyespt_PT
dc.publisherElsevierpt_PT
dc.rights.urihttp://creativecommons.org/licenses/by/4.0/pt_PT
dc.subjectBacterial nanocellulosept_PT
dc.subjectGluconacetobacter xylinuspt_PT
dc.subjectHybrid bio-nanocompositespt_PT
dc.subjectCaCO3pt_PT
dc.subjectIn situ biosynthesispt_PT
dc.subject.pt_PT
dc.subjectFaculdade de Ciências Exatas e da Engenhariapt_PT
dc.titleIn situ biosynthesis of bacterial nanocellulose-CaCO3 hybrid bionanocomposite: one-step processpt_PT
dc.typejournal article
dspace.entity.typePublication
oaire.citation.endPage399pt_PT
oaire.citation.startPage393pt_PT
oaire.citation.titleMaterials Science and Engineering: Cpt_PT
oaire.citation.volume65pt_PT
person.familyNameFaria
person.familyNamecordeiro
person.givenNameMarisa Camacho Gonçalves
person.givenNamenereida
person.identifier1612636
person.identifier.ciencia-idD716-6F48-AD0E
person.identifier.ciencia-id521A-0F62-EA39
person.identifier.orcid0000-0002-9158-6961
person.identifier.orcid0000-0001-6006-3415
person.identifier.ridO-2253-2019
person.identifier.scopus-author-id7004319456
rcaap.rightsopenAccesspt_PT
rcaap.typearticlept_PT
relation.isAuthorOfPublication57ef72f0-8e40-4853-b4ab-416884e127fa
relation.isAuthorOfPublication3d02b657-c48c-4f56-813a-1284b81960f3
relation.isAuthorOfPublication.latestForDiscovery57ef72f0-8e40-4853-b4ab-416884e127fa

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