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Microextraction by packed sorbent: an emerging, selective and high-throughput extraction technique in bioanalysis

2014Journal article Restricted access
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dc.contributor.authorPereira, Jorge
dc.contributor.authorCâmara, José S.
dc.contributor.authorColmsjö, Anders
dc.contributor.authorAbdel-Rehim, Mohamed
dc.date.accessioned2019-07-19T10:23:18Z
dc.date.available2019-07-19T10:23:18Z
dc.date.issued2014
dc.description.abstractSample preparation is an important analytical step regarding the isolation and concentration of desired components from complex matrices and greatly influences their reliable and accurate analysis and data quality. It is the most labor-intensive and error-prone process in analytical methodology and, therefore, may influence the analytical performance of the target analytes quantification. Many conventional sample preparation methods are relatively complicated, involving time-consuming procedures and requiring large volumes of organic solvents. Recent trends in sample preparation include miniaturization, automation, high-throughput performance, on-line coupling with analytical instruments and low-cost operation through extremely low volume or no solvent consumption. Micro-extraction techniques, such as micro-extraction by packed sorbent (MEPS), have these advantages over the traditional techniques. This paper gives an overview of MEPS technique, including the role of sample preparation in bioanalysis, the MEPS description namely MEPS formats (on- and off-line), sorbents, experimental and protocols, factors that affect the MEPS performance, and the major advantages and limitations of MEPS compared with other sample preparation techniques. We also summarize MEPS recent applications in bioanalysis.pt_PT
dc.description.versioninfo:eu-repo/semantics/publishedVersionpt_PT
dc.identifier.citationPereira, J., Câmara, J. S., Colmsjö, A., & Abdel‐Rehim, M. (2014). Microextraction by packed sorbent: an emerging, selective and high‐throughput extraction technique in bioanalysis. Biomedical Chromatography, 28(6), 839-847.pt_PT
dc.identifier.doi10.1002/bmc.3156pt_PT
dc.identifier.issn0269-3879
dc.identifier.urihttp://hdl.handle.net/10400.13/2486
dc.language.isoengpt_PT
dc.peerreviewedyespt_PT
dc.publisherJohn Wiley and Sonspt_PT
dc.relationStrategic Project - UI 674 - 2011-2012
dc.subjectMicro extraction techniques (μET)pt_PT
dc.subjectMicro extraction by packed sorbent (MEPS)pt_PT
dc.subjectSorbentspt_PT
dc.subjectApplicationspt_PT
dc.subjectFuture trendspt_PT
dc.subject.pt_PT
dc.subjectFaculdade de Ciências Exatas e da Engenhariapt_PT
dc.subjectCentro de Química da Madeira
dc.titleMicroextraction by packed sorbent: an emerging, selective and high-throughput extraction technique in bioanalysispt_PT
dc.typejournal article
dspace.entity.typePublication
oaire.awardTitleStrategic Project - UI 674 - 2011-2012
oaire.awardURIinfo:eu-repo/grantAgreement/FCT/6817 - DCRRNI ID/PEst-OE%2FQUI%2FUI0674%2F2011/PT
oaire.citation.endPage847pt_PT
oaire.citation.startPage839pt_PT
oaire.citation.titleBiomedical Chromatographypt_PT
oaire.citation.volume28(6)pt_PT
oaire.fundingStream6817 - DCRRNI ID
person.familyNameAugusto Machado Pereira
person.familyNameCâmara
person.familyNameAbdel-Rehim
person.givenNameJorge
person.givenNameJosé
person.givenNameMohamed
person.identifierG-3003-2013
person.identifier.ciencia-idEC12-EE8F-50E8
person.identifier.ciencia-id481C-08CE-90E5
person.identifier.orcid0000-0003-0316-5348
person.identifier.orcid0000-0003-1965-3151
person.identifier.orcid0000-0002-3862-8878
person.identifier.scopus-author-id10140393000
person.identifier.scopus-author-id7003923945
project.funder.identifierhttp://doi.org/10.13039/501100001871
project.funder.nameFundação para a Ciência e a Tecnologia
rcaap.rightsrestrictedAccesspt_PT
rcaap.typearticlept_PT
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relation.isAuthorOfPublicatione10d78be-e547-4d25-92b5-06a997ed78da
relation.isAuthorOfPublicationc039efd6-bafa-420a-bf90-bbd00da090b0
relation.isAuthorOfPublication.latestForDiscoverye10d78be-e547-4d25-92b5-06a997ed78da
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